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NEW RECORD SET FOR SMALLEST X-RAY NANO-SPOT
01 March 2007 - DOE/Argonne National Laboratory

An award-winning device developed at the U.S. Department of Energy's Argonne National Laboratory has set a world's record for tiny spot size with a hard X-ray beam.

The lens, just like the lens of a camera, allows precise focusing of the X-ray light.Using the lens, researchers will be able to visualize three-dimensional electronic circuit boards to find circuit errors, or map impurities in biological or environmental samples at the nanometer scale. They can also analyze samples inside high-pressure or high-temperature cells, since hard X-rays, unlike soft X-rays, are able to penetrate container walls.

Other examples of uses of the new lens include development of smaller, better-performing and more reliable computers and telecommunications equipment; improving materials for energy efficient lighting, motors, fuel cells and solar energy production; production of lighter, sturdier, safer transportation vehicles through advanced materials with tailored properties; imaging cell division and tumor growth, providing a new mechanism for the early detection of cancer; and faster, more sensitive detection of hazards in local and global environments.

The researchers developed the record-setting lens by depositing 728 layers of material, one layer at a time, on a silicon substrate wafer. The thickness of the layer stack, when completed, was 12.4 microns. The wafer is then sectioned into bars that are used to make the lenses for the X-ray.

The work is published in today's edition of Physical Review Letters.

“The accomplishment here is two-fold,” said lead author Hyon Chol Kang. “The first is to grow that many layers without peeling, and, second, to cut and polish a bar without damaging the lens. We're continuing the development, and calculations for an idealized structure indicate that a focus of one nanometer is not prohibited by any known physics. The great challenge will be to grow the idealized structure.”

The optical design is akin to a linear Fresnel lens conventionally made by photolithography, but with the crucial difference that the diffraction structure is formed from many individually sputtered layers. High quality sputtered layers can be grown with thicknesses of 1 nm, and it is this control which makes the multilayer lens possible.

The new device is being used at the Advanced Photon Source at Argonne, which produces the most brilliant X-rays in the Western Hemisphere. It will also be particularly useful as the Center for Nanoscale Materials at Argonne becomes operational later this year.

Researchers Al Macrander, Chian Liu and Raymond Conley, all part of the Advanced Photon Source Experimental Facilities Division optics fabrication and metrology group, developed the lens wafers. They are joined by Stefan Vogt, also of the Experimental Facilities Division; Kang and Brian Stephenson of the Materials Science Division at Argonne, and Jorg Maser of the Accelerator Systems Division at Argonne. The work is especially meaningful for Maser, who predicted the theoretical ability of an X-ray lens to focus at this small size in his doctoral dissertation in 1994.

The nation's first national laboratory, Argonne National Laboratory conducts basic and applied scientific research across a wide spectrum of disciplines, ranging from high-energy physics to climatology and biotechnology. Since 1990, Argonne has worked with more than 600 companies and numerous federal agencies and other organizations to help advance America's scientific leadership and prepare the nation for the future. Argonne is managed by UChicago Argonne, LLC for the U.S. Department of Energy's Office of Science.

http://www.anl.gov

About: DOE/Argonne National Laboratory
Argonne National Laboratory is one of the US Department of Energy's largest research centres. It is also the nation's first national laboratory, chartered in 1946.

Argonne is a direct descendant of the University of Chicago's Metallurgical Laboratory, part of the World War Two Manhattan Project. After the war, Argonne was given the mission of developing nuclear reactors for peaceful purposes. Over the years, Argonne's research expanded to include many other areas of science, engineering and technology.

Today, the laboratory has about 4000 employees, including about 1200 scientists and engineers, of whom about 700 hold doctorate degrees.

Argonne occupies two sites. The Illinois site is surrounded by forest preserve about 25 miles southwest of Chicago's Loop. About 3200 of Argonne's 4000 employees work on the site's 1500 wooded acres. The site also houses the US Department of Energy's Chicago Operations Office.

Argonne-West occupies about 900 acres about 50 miles west of Idaho Falls in the Snake River Valley. It is the home of most of Argonne's major nuclear reactor research facilities. About 800 of Argonne's employees work there.


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